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What is the difference between distillation, distillation under reduced pressure and steam distillation ?

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प्रश्न

What is the difference between distillation, distillation under reduced pressure and steam distillation ?

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उत्तर

The differences among distillation, distillation under reduced pressure, and steam distillation are given in the following table.

Distillation Distillation under
reduced pressure
Steam distillation
It is used for the purification of compounds that are associated with non-volatile impurities or those liquids, which do not decompose on boiling. In other words, distillation is used to separate volatile liquids from non-volatile impurities or a mixture of those liquids that have sufficient difference in boiling points. This method is used to purify a liquid that tends to decompose on boiling. Under the conditions of reduced pressure, the liquid will boil at a low temperature than its boiling point and will, therefore, not decompose. It is used to purify an organic compound, which is steam volatile and immiscible in water. On passing steam, the compound gets heated up and the steam gets condensed to water. After some time, the mixture of water and liquid starts to boil and passes through the condenser. This condensed mixture of water and liquid is then separated by using a separating funnel.
Mixture of petrol and kerosene is separated by this method. Glycerol is purified by this method. It boils with decomposition at a temperature of 593 K. At a reduced pressure, it boils at 453 K without decomposition. A mixture of water and aniline is separated by steam distillation.
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पाठ 8: Organic Chemistry - Some Basic Principles and Techniques - EXERCISES [पृष्ठ ३७१]

APPEARS IN

एनसीईआरटी Chemistry - Part 1 and 2 [English] Class 11
पाठ 8 Organic Chemistry - Some Basic Principles and Techniques
EXERCISES | Q 12.20 | पृष्ठ ३७१

संबंधित प्रश्‍न

How will you separate a mixture containing kerosene and petrol (difference in their boiling points is more than 25°C), which are miscible with each other?


How would you confirm that a colourless liquid given to you is pure water?


Give a brief description of the principle of the following technique taking an example.

Distillation 


Explain the difference between Separation by distillation and by separating funnel. 


Pure water from impure water

  • Give the principle involved in the separation of the mixture
  • Give the technique of separation of the mixture.

Choose the correct option.

Which of the following methods can be used to separate two compounds with different solubilities in the same solvent?


Choose the correct option.

Which of the following techniques is used for the separation of glycerol from soap in the soap industry?


Choose the correct option.

A mixture of acetone and benzene can be separated by the following method:


What will happen if the upper outlet of the condenser is connected to the tap instead of the lower outlet?


Define Distillation


Alcohol can be separated from water by ______.


Which of the tubes in Fig. 2.1 (a) and (b) will be more effective as a condenser in the distillation apparatus?


Match the type of mixture of compounds in Column I with the technique of separation/purification given in Column II.

Column I Column II
(i) Two solids which have different solubilities in a solvent and which do not undergo reaction when dissolved in it. (a) Steam distillation
(ii) Liquid that decomposes at its boiling point (b) Fractional distillation
(iii) Steam volatile liquid (c) Simple distillation
(iv) Two liquids which have boiling points close to each other (d) Distillation under reduced pressure
(v) Two liquids with large difference in boiling points. (e) Crystallisation

Draw a diagram of bubble plate type fractionating column. When do we require such type of a column for separating two liquids. Explain the principle involved in the separation of components of a mixture of liquids by using fractionating column. What industrial applications does this process have?


Explain the factors, which will affect the rate of evaporation, taking examples from our daily life experiences.


What is distillation?


A mixture of benzene and chloroform is separated by ______.


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